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KMID : 1036420140070020049
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2014 Volume.7 No. 2 p.49 ~ p.57
Effect of Different Surface Treatment on the Shear Bond Strength between Yttria-Tetragonal Zirconia Polycrystal and Non-10-Methacryloyloxydecyl Dihydrogen Phosphate-Containing Resin Cement
Lee Yoon

Yi Young-Ah
Kim Sin-Young
Seo Deog-Gyu
Abstract
Purpose: To evaluate the effect of different surface treatment methods (yttria-tetragonal zirconia polycrystal [Y-TZP] primers, air-abrasion, and tribochemical surface treatment) on the shear bond strength between (Y-TZP) ceramics and etch-and-rinse non-10-methacryloyloxydecyl dihydrogen phosphate (MDP)-containing resin cements.

Materials and Methods: Y-TZP ceramic surfaces were ground flat with 600-grit silicone carbide abrasives paper and then divided into seven groups of ten. They were treated as the following: untreated (control), Monobond Plus (IvoclarVivadent), Z-PRIME Plus (Bisco Inc.), ESPE Sil with CoJet (3M ESPE), air-abrasion, Monobond Plus with air-abrasion, and Z-PRIME Plus with air-abrasion. The surface of Y-TZP specimens was analyzed under a scanning electron microscope (SEM). Non-MDP-containing cements were placed on the surface-treated Y-TZP specimens. After thermocycling, shear bond strength test was performed. Bond strength values were statistically analyzed using one-way analysis of variance and Student-Newman-Keuls multiple comparison test (P<0.05).

Result: The Z-PRIME Plus treatment in combination with air-abrasion produced the highest bond strength (14.94¡¾1.70 MPa) followed by Monobond Plus combined with air-abrasion (10.70¡¾1.71 MPa), air-abrasion (10.47¡¾1.60 MPa), ESPE Sil after CoJet treatment (10.38¡¾0.87 MPa), Z-PRIME Plus application (10.00¡¾1.70 MPa), and then Monobond Plus application (9.25¡¾0.86 MPa). The control (6.70¡¾1.49 MPa) indicated the lowest results (P<0.05). The SEM results showed different surface morphologies according to surface treatment methods compared with the Y-TZP control.

Conclusion: The shear bond strength between the Y-TZP ceramic and the non-MDP-containing resin cement was the greatest when the surface was treated with air-abrasion and MDP-containing Z-PRIME Plus primer.
KEYWORD
Bond strength, Primer, Resin cements, Surface treatment, Yttria-tetragonal zirconia polycrystal ceramic
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